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Study on the Synthetic Process of 4-N, N-dimethylaminothiobenzoic Acid
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WANG Rui , XIE Kaijun, LI Zhenghao, FAN Feilong, WANG Zhenxuan, FU Qiang, PAN Gaofeng
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 1-5.
doi:10.16039/j.cnki.cn22-1249.2022.07.001
The process of synthesizing 4-N, N-dimethylaminothiobenzoic acid (DMATBA) with 4-N,N-dimethylaminobenzoyl chloride and NaHS as raw materials was studied, involving the influence of the type of reaction solvent, reaction concentration, n (NaHS): n (4-N,N-dimethylaminobenzoyl chloride) feed ratio, reaction time, reaction temperature and n (NaHS): n (HCl) dosage ratio on the yields of the product. The effects of solvent type, reaction concentration, n (NaHS) : n (4-N, N-Dimethylaminobenzyl Chloride) feeding ratio, reaction time, reaction temperature, n (NaHS) : n (HCl) dosage ratio of on product yield were investigated. Experimental results show that the best synthesis process in this screen involved reaction solvent DMF, reaction concentration 1.0 mol/L, n (NaHS): n (4-N,N-dimethylaminobenzoyl chloride) = 2:1, reaction time 2.5 h, reaction temperature 25 oC, n (NaHS): n (HCl) = 1:1 (PH = 3); after acidification, extraction, and vacuum distillation, the total yield of DMATBA can reach 82.1%, and the purity is 93.6%.
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Direct Contact Membrane Distillation to Treat Wig Wastewater
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PANG Erxi, , SUN Guofu , WANG Weidong, , XU Jingli
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 12-17.
doi:10.16039/j.cnki.cn22-1249.2022.07.003
The process of membrane distillation to aim at treating the wig wastewater was designed.The effects of feed temperature, feed flow rate, feed pH, surfactant concentration in feed, running time on permeation flux and rejection of direct contact membrane distillation (DCMD) were investigated. Meanwhile, the contaminated membrane was characterized and cleaned. The results showed that the permeation flux is about 66 kg/m2·h and the rejection rate is above 99.25% after running for 100 hours under the condition that the feed temperature is 60 ℃, the feed flow rate is 120 L/h, the cooling water flow rate is 60 L/h, and the feed pH is 1.48. The pH of the produced water was 6.82, COD and TDS are not detected. The produced water meets the regulations of the emission. It is feasible to treat the wig treatment by DCMD.
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Optimization Design of PID Controller based on Particle Swarm Optimization Algorithm
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Dong ruyi, Tang yuyu, Sang keke
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 18-21.
doi:10.16039/j.cnki.cn22-1249.2022.07.004
In view of the classic particle swarm algorithm in PID controller parameter setting method of its effect is often poor, this paper puts forward an improved particle swarm algorithm optimization design of the PID controller parameter setting, on the basis of the particle swarm to join the crossover operator of genetic algorithm, and the particle swarm of inertia weight factor into a dynamic parameter, The applied PID controller improves the adaptive tuning of parameters, and the rapidity and stability are better than those of the classical PSO PID controller. With the help of Matlab to simulate the response curve of the system, according to the comparison of the system performance index improvement.
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Active disturbance rejection control for liquid level of double tank based on PLC
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MENG YaNan , ZHANG Zhenhuai
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 22-27.
doi:10.16039/j.cnki.cn22-1249.2022.07.005
In people's life and some industrial production, will involve the problem of liquid level control, but the water tank level is often automatic control effect is not good. This paper first introduces the status quo of water tank level control and control deficiencies, and then carries on the design of active disturbance rejection controller, based on the traditional PID combined with active disturbance rejection control technology. Secondly, the hardware system of this design system is designed and selected. Finally, through the lower computer programming, upper computer state, program running and upper computer screen monitoring and experimental results analysis, the control system has achieved the automatic control effect of water tank liquid level has been greatly improved.
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Design of Water Surface Floating Object Recognition Algorithm based on Deep Learning
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LIU qi , YIN Gang , WANG ying , YE Ze
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 28-33.
doi:10.16039/j.cnki.cn22-1249.2022.07.006
For the difficult problem of small water floating object recognition, a deep learning-based target recognition method is improved. In this paper, an improved YOLOv5s target recognition algorithm is used to recognize water floating objects. First, according to the characteristics of the shape of floating objects on the water surface, the improved K-means algorithm is used to re-cluster the anchor boxes, then, Squeeze-and-Excitation networks module is added and then α-IOU is applied to the YOLOv5s network. The experimental results show that, compared with the standard YOLOv5s algorithm, the precision and average precision of the improved YOLOv5s algorithm are increased by 2% and 4% respectively, which verifies the effectiveness of the algorithm. This method can overcome the influence of water surface environment and effectively identify floating objects on the water surface.
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Path Planning and Following of Mobile Robots in Complex Environments
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WANG Ying, YANG Jiaxin, LIU Qi, XU Jiaojiao
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 34-41.
doi:10.16039/j.cnki.cn22-1249.2022.07.007
This paper proposed a new path planning and path following control method for mobile robots based on improved A* algorithm and PID control algorithm, which is suitable for complex maze environments. In the proposed method, the problem of too many turning points of the A* algorithm is solved, and the generated expected path is safe and smooth by extending the obstacles and the fourth-order cubic uniform B-spline optimization method. Afterwards, a PID controller is designed based on the kinematic model of the two-wheel differential robot based on the forward viewpoint. The performance of the proposed method is tested in a specially designed framework. As a verification, detailed experiments are carried out from the two aspects of path planning and path following. The results show that the planning path has few turning points and the path is smooth, and the designed PID controller can control the mobile robot to achieve better path following effect. Finally, the proposed method is validated in a complex maze environment, and the results show that the proposed method enables the robot to traverse the maze without collision.
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Research on Backstepping Sliding Mode Control for Ball and Plate System with Command Filter
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MENG Shengjun, HAN Guangxin, BAI Haowen, Lu Yingxin
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 42-48.
doi:10.16039/j.cnki.cn22-1249.2022.07.008
In order to solve the problem that the chattering phenomenon in sliding mode control affects the trajectory tracking control performance of the ball and plate system, backstepping sliding mode control method combined with a command filter is proposed. Firstly, the mathematical model of the ball and plate system is established, and the general sliding mode control law is designed according to the system error equation. Secondly, a compound system with command filter is constructed and an error backstepping controller is designed. Finally, the global asymptotic stability of the whole closed-loop system is proved by Lyapunov theory. The simulation results show that this method can effectively suppress the chattering phenomenon and further strengthen the disturbance-rejection performance.
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Research on Dynamic Matrix Control of Liquid Level in Single Tank
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GUO Xiaonan, XU Zhaolian, ZHANG Longqin, CAO Yubo
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 58-61.
doi:10.16039/j.cnki.cn22-1249.2022.07.011
Aiming at the problem of constant water level control of water tank level, the dynamic mathematical model of single tank is established by mechanism analysis method. The dynamic matrix control algorithm is a single tank liquid level predictive control algorithm. Taking the state equation of liquid level as the prediction model, a dynamic matrix controller is designed and implemented. At present, the constant water level control of water tank liquid level is realized. The simulation results show that the proposed dynamic matrix control algorithm for liquid level of single tank has fast response speed, short adjustment time, strong anti-interference ability and good control effect.
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Clustering Algorithm based on Evolutionary Thought and Its Cluster Fusion Algorithm
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SHI Yanli, JIN Huan
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 77-85.
doi:10.16039/j.cnki.cn22-1249.2022.07.015
Aiming at the defects of K-means clustering algorithm that the number of clusters is unknown in advance and cannot deal with non-convex distributed data sets, a clustering algorithm based on evolutionary idea and its cluster fusion algorithm are proposed, The algorithm embeds the K-means clustering algorithm into the framework of evolutionary clustering algorithm. By adjusting the distance doubling parameter, the data objects will be divided gradually, and the number of clusters k will be determined adaptively, Then, a middle circle density cluster fusion algorithm based on the nearest distance and a middle circle density cluster fusion algorithm based on representative classes are proposed to fuse the clusters with high similarity, so that the k value gradually tends to the real value. Experiments show that this method has good practice.
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Study on Sudden Vibration Fault Identification of High and Intermediate Pressure Rotor of Steam Turbine in Power Plant
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ZENG Na
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 94-99.
doi:10.16039/j.cnki.cn22-1249.2022.07.018
In order to ensure the safe and stable operation of the power plant steam turbine in the high temperature and high speed environment, a sudden vibration fault identification method of high and intermediate pressure rotor of steam turbine in power plant is proposed. According to the shafting vibration characteristics of the high and medium pressure rotor vibration of the power plant turbine, the integrated eddy current displacement sensor is used to collect the corresponding fault signal, and the wavelet packet analysis is used to extract the high and medium pressure rotor vibration mutation fault characteristics, and the extracted fault characteristics are used as input. Input the fault features into the RBF neural network optimized by artificial fish swarm algorithm, and output the identification result of the vibration mutation type of the high and medium pressure rotor of the steam turbine of the power plant. During the experiment, the method in this paper was used to identify 9 common faults, such as mass unbalance, rotor thermal bending, shaft misalignment, rotating parts flying off, dynamic and static friction, steam flow excitation, structural resonance, insufficient structural rigidity, and rotor cracks. The experimental results show that the method decomposes and reconstructs the high-pressure rotor vibration mutation fault signal of the power plant steam turbine with high quality, and the obtained fault identification result is the same as the actual fault, the identification accuracy is high, and the result is reliable.
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A Nursing Bed with Fast Folding Function
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ZHOU Haodong, XIAO Tong, CHEN Youguang, REN Shujuan, CHU Yaxu, LV Jinhe, LI Hongzhou
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 100-105.
doi:10.16039/j.cnki.cn22-1249.2022.07.019
In response to emergencies such as infectious disease outbreaks and the practical needs of multi-functional nursing beds, a new multi-functional nursing bed was designed and developed. For rapid treatment and nursing, this nursing bed can realize the functions of lifting back, cleaning stool and folding bed body.Using SolidWorks for 3D modeling, through ANSYS Workbench for 3d model simulation analysis, get the motion curve of each mechanism and bed plate force cloud, proved the rationality of the design of each mechanism and the stability of the bed body.
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Optimum design of clamping jaws for welding fixture of exhaust pipe
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PAN Zhikui, CHEN Xue
Journal of Jilin Institute of Chemical Technology, 2022, 39(7): 106-110.
doi:10.16039/j.cnki.cn22-1249.2022.07.020
Using the finite element software ANSYS Workbench, the static analysis of the clamping jaws of the exhaust pipe welding fixture clamping mechanism was carried out, and the deformation and stress distribution of the clamping jaws were obtained. On the premise that the gripper meets the strength and stiffness requirements of exhaust pipe welding, the size of the gripper is optimized by the response surface optimization method in multi-objective optimization. First, the mathematical model of gripper optimization is established, and the objective function and constraints are set. Conditions, and then parameterize each size of the gripper, and obtain the coptimal design size of the gripper by calculation. The topological optimization of the jaw structure is then carried out by the variable density method to reduce its mass. Comparing the deformation and stress distribution before and after optimization of the clamping jaw the results show that the weight of the campina jaw is reduced by 27.9% when the stress and deformation meet the design requirements after the optimization.
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