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An Efficient Synthesis of Ginsenoside Rg5 Via Conversion from Ginseng Fibrous Root Powder in the Presence of Molecular Sieves
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YE Anqi, ZHANG Haoran, ZHANG Yuewei, LI Ling, CHENG Leqin
Journal of Jilin Institute of Chemical Technology, 2021, 38(3): 1-6.
doi:10.16039/j.cnki.cn22-1249.2021.03.001
The rare ginsenoside Rg5 was efficiently prepared in the presence of molecular sieves. using the multi-functional improved Soxhlet extractor as extraction tool and ginseng fibrous root powder as raw material, hydrochloric acid as catalyst. The extraction process of ginsenoside Rg5 was optimized through one-factor experiment. The optimum result obtained from one-factor test was as follows: extraction solvent was 30 mL methanol, 4A molecular sieve was 0.3 g, the heating temperature in the extraction barrel was 65 ℃, and extraction time was 4 h. Under the optimized conditions, the extraction yield of total ginsenosides reached 10.2% and the yield of rare ginsenoside Rg5 was 3.20%, which could significantly improve the preparation efficiency of ginsenoside Rg5 compared with the traditional Soxhlet extractor. The method has following characteristics such as high extraction yield and simple operation, which indicated the method could extract Rg5 effectively.
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Optimization of Determination Method of Lead in Angelica Based on Box-Behnken Desig
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WANG Zhaoguo
Journal of Jilin Institute of Chemical Technology, 2021, 38(3): 7-12.
doi:10.16039/j.cnki.cn22-1249.2021.03.002
The absorbance of lead in flour was determined by microwave digestion method and atomic absorption spectrophotometer. Box-behnken Design was used to determine the best instrumental analysis conditions. Through the single-factor test, the four factors of ashing temperature, ashing time, atomization temperature and atomization time were selected for the three-level test. The mathematical model was established by Box-Behnken Design, and the optimal conditions were sought by variance analysis, response surface analysis and desire function optimization. Results show that the established mathematical model of the R2=0.9671,R2Adj =0.9342 shows that the model has good credibility, this model could be used to predict the coefficient of variation CV % = 3.08%, indicates that under the condition of the experiment, variation is small, the model has good repeatability, when ashing temperature is 525℃, ashing time is 20s, atomization temperature is 1550℃, atomization time for 5s absorbance maximum 0.24; Therefore, this study can provide a good theoretical basis for the determination of lead by atomic absorption spectrophotometer.
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Influence of Medium Pressure and O-ring Compression Rate on Performance of Reciprocating Shaft Seal
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WANG Lin, CHEN Qing, ZOU Xinhuan, LIU Jindong, SHI Long, JIANG Ziwei
Journal of Jilin Institute of Chemical Technology, 2021, 38(3): 16-21.
doi:10.16039/j.cnki.cn22-1249.2021.03.004
Taking the O-shaped rubber ring in the reciprocating seal of the Hydraulic cylinder as the research object, a two-dimensional axisymmetric model was established. With a friction coefficient of 0.1, different medium pressures and different pre-compression ratios, the finite element software ANSYS workbench is used to analyze the deformation and stress of the O-ring during installation, static pressure and working conditions. The results indicate that: when the compression rate exceeds 15% during reciprocating motion, it is easy to cause O-ring stress relaxation, compression permanent deformation, and loss of sealing ability; and the seal ring has the most obvious stress concentration in the gap between the cylinder and the piston rod. In this position, it is easy to be squeezed into the gap, causing gap bite, resulting in seal failure; in the case of oil pressure less than 15MPa, the shear stress is always less than the shear strength of nitrile rubber, but under the reciprocating movement, the sealing ring will continue to It is easy to accumulate damage by friction and wear, leading to cracks or damage.
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A Study of the Effect of Fuel Nozzle Structural Parameters on Cavitation Performance
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LU Hongjie, GAN Shukun, LV Xuefei
Journal of Jilin Institute of Chemical Technology, 2021, 38(3): 22-26.
doi:10.16039/j.cnki.cn22-1249.2021.03.005
Cavitation in the diesel nozzle can have a serious impact on the performance of the diesel engine. On the one hand, it promotes the atomisation of the fuel, enabling efficient and sufficient combustion of the fuel inside the engine and reducing the possibility of carbon build-up. On the other hand cavitation can cause cavitation wear inside the nozzle, thus affecting the life and performance of the nozzle. This paper investigates the effect of nozzle structural parameters on cavitation performance through computational fluid dynamics using a VOF model plus a cavitation model. Three dimensionless quantities, the gas-liquid inlet angle ratio, the gas-liquid inlet length ratio, and the gas-liquid inlet diameter ratio, are analysed using the dimensionless quantity method. To provide a theoretical basis for future research into the fuel atomisation characteristics of gas-liquid two-phase fuel nozzles.
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6~10KV Line Overcurrent Protection Laboratory Simulation and Multisim Simulation Realization
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CHEN Xudong, TAN Xiaojing
Journal of Jilin Institute of Chemical Technology, 2021, 38(3): 37-43.
doi:10.16039/j.cnki.cn22-1249.2021.03.008
Based on the basic principle of 6~10KV line over-current protection, design the on-site simulation realization under laboratory conditions and the simulation realization on the Multisim software platform. In the laboratory field simulation design, the principle wiring diagram-expand the wiring diagram-the design idea of the experimental wiring diagram, equipment selection and connection, a detailed equipment list and operation process, and finally recorded experimental simulation data. In the simulation design of the Multisim software platform, the field simulation experimental wiring diagram is the design basis Design the simulation circuit, and the equipment selection focuses on the presentation of functions. The connection structure of the equipment can be adjusted appropriately without affecting the actual function, and the simulation can be carried out in accordance with the on-site simulation operation sequence.The realization of virtual simulation must be based on the laboratory simulation data, and the two cooperate with each other , Learn from each other to achieve better teaching and learning results.
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Reverse Self-cleaning Sweeper Structural Design
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LIU Ronghui
Journal of Jilin Institute of Chemical Technology, 2021, 38(3): 44-47.
doi:10.16039/j.cnki.cn22-1249.2021.03.009
Based on the analysis of the structural characteristics of the existing sweeper, a sweeper with simple structure and high cleaning quality is designed. In this paper, the system composition and working principle of the sweeper are discussed in detail, including cleaning mechanism, reverse cleaning mechanism, filtration device, spraying self-cleaning device, walking mechanism, lifting mechanism, auxiliary mechanism, etc., in order to provide technical reference for the design of the small sweeper.
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Design of Skiing Posture Training Simulator Based on VR
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LI Yanlong, CHEN Xue, XU Zhaoyang, YANG Hu, CHEN Yangyang, XIA Rurui, WANG Mingyang
Journal of Jilin Institute of Chemical Technology, 2021, 38(3): 48-51.
doi:10.16039/j.cnki.cn22-1249.2021.03.010
Skiing is a popular winter sport. In order to realize the beginner's quick start and the simulation of skiing process, an indoor skiing posture training simulator based on VR is designed. The simulator consists of three parts: virtual simulation system, sports training system and safety protection system, VR virtual simulation system can simulate the skiing training scene and increase the reality of skiing; the sports training system includes a variety of institutions to maximize the simulation of skiing posture; the safety protection system can protect users; the trainer combined with VR technology can realize the multi-dimensional simulation of skiing posture under the real skiing scene experience, so that the skier can experience the real body feeling when simulating the sports, and improve the real scene feeling of the experience person simulating skiing significantly.
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Research on Access Strategy of Stacked Stereo Garage Based on Roadway
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LIU qi, ZHANG Ye, WANG ying, Xu Jiaojiao, LI Baohua, GOU yao
Journal of Jilin Institute of Chemical Technology, 2021, 38(3): 67-69.
doi:10.16039/j.cnki.cn22-1249.2021.03.014
Is common in urban and rural residential parking problems such as insufficient parking Spaces, access time is too long, in order to improve the vehicle's access policy, vehicle access time as objective function, using the queuing theory, respectively, set up priority save car, first car, sequential access, interleaved, such as the mathematical model of different routes, the working efficiency of the different access strategy to make use of the MATLAB simulation calculation, through contrast to choose the appropriate access strategy, the ideal way of access strategy, improve the utilization rate of parking Spaces and effectively solved the three-dimensional garage the existing problems, and widely used.
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Effects of the substrate ratio on cutting of Tibouchina aspera
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LIU Xiaoli, TANG Wenli, BIAN Jingjing, HE Xuecheng
Journal of Jilin Institute of Chemical Technology, 2021, 38(3): 82-86.
doi:10.16039/j.cnki.cn22-1249.2021.03.017
Tibouchina aspera is an excellent ornamental plant in Landscape ar-chitecture. In this paper, based on a 30-day cutting experiment, the effects of different substrate ratios on the growth of the cuttings of Paeonia suffruticosa were compared, and the rooting time, root number, longest root length, rooting rate, growth state of cuttings and substrate changes were analyzed. The results show the ratio of treatment group T8 (original soil: fine sand: peat soil: vermiculite: perlite) = 1: 1: 2: 1: 1 has the fastest rooting rate of cuttings, longest root length and best cutting growth among all experimental treatment groups. The treatment effect of T (peat soil) comes second, and it can be used as a backup plan for production under limited conditions.
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Features of Probability Theory and Its Implementation Strategies
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Liu Bin, Yuan Yunyun, Niu Xiangyang
Journal of Jilin Institute of Chemical Technology, 2021, 38(3): 91-96.
doi:10.16039/j.cnki.cn22-1249.2021.03.019
The method of probability theory is a specific strategy to analyze, dispose and solve the problems of probability theory, with its features of randomness, generality, hierarchy, pertinence, integration and manipulity. The strategy of efficient implementation of probability theory is to clarify problems through association to bridge the known and unknown channels; to acquire construction through common models to solve problems directly or indirectly; to be reflective through review to refine innovation on probability models and methods.
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