|
Study on of the Theextraction Technology of Proanthocyanidin by Ultrasonic Assisted Methanol
Collect
ZHU Bo, LIU Shan-shan
Journal of Jilin Institute of Chemical Technology, 2019, 36(1): 1-4.
doi:10.16039/j.cnki.cn22-1249.2019.01.001
The extraction technology of proanthocyanidin from Crataegus pinnatifida Bunge by ultrasonic assisted methanol was investigated in this paper. Four different factors: extraction temperature, extraction time, solvent concentration, solid-liquid ratio were selected in Orthogonal experiment. The most optimal conditions were confirmed as concentration 70%, extraction temperature 60℃, solid-liquid ratio 1:15, extraction time 30 min, and the extraction yield of proanthccyanidins from Crataegus pinnatifida Bunge reached to 1.781%.
Related Articles |
Metrics
|
|
Study of Optimum Conditions on Supercritical CO2Fluild Extraction of Spent Auricularia Auricula Substrate
Collect
WANG Zong-yong, ZHAO Yi, HE Miao, YANG Hui-ru, LI Ping, XUE Xiao-li
Journal of Jilin Institute of Chemical Technology, 2019, 36(1): 5-10.
doi:10.16039/j.cnki.cn22-1249.2019.01.002
Objective: The optimum conditions for the extraction of Spend Auricularia auricular substrate by supercritical CO2 fluid were studied, and the chemical composition of the extract was analyzed. Methods: Taking the extraction rate as the indicator, orthogonal test of L9 (34) with four factors and three levels was carried out to determine the best conditions on the basis of single factor experiment. The extraction was analyzed with gas chromatograph/mass spectrometer. Results: The results showed that the optimal extraction conditions were 30 MPa, 45 ℃, 60 mesh, 400 mL of the entrainer volume and the extraction rate was 3.25% under these conditions. The chemical composition of extraction can be classified into alcohols, ethers, aldehydes, ketones, organic acids, esters, terpenoids, steroids. The three most abundant compounds were methyl linoleate (5.56%), 17β(H),21β(H)-hop-22(29)-EN-3-one(5.26%),3,5-cholestanedien-7-one(4.05%),respectively. Conclusion: Extraction and separation of fine chemicals from spend auricularia auricular substrate is a new idea of clean and efficient utilization of biomass.
Related Articles |
Metrics
|
|
Preparation and Quality Evaluation of Total Triterpenoid Saponins Hard Capsule from Orostachys fimbriatus (Turcz) Berger
Collect
ZHOU Ming, WANG Ya-hong, CHU Xu
Journal of Jilin Institute of Chemical Technology, 2019, 36(1): 21-24.
doi:10.16039/j.cnki.cn22-1249.2019.01.005
The preparation technology, quality evaluation of total triterpenoid saponins hard capsule from Orostachys fimbriatus (Turcz) Berger were discussed in this paper. Taking the moisture absorption rate and the angle of repose as the indicators, the best excipients and amount of auxiliary materials were selected, and the bulk density was used to determine the capsule loading, determine the relative critical humidity of filling capsules by using moisture absorption rate as an indicator. In the process of quality inspection, the disintegration time and moisture content of hard capsules were examined.The preparation process conditions of the total triterpenoid saponins hard capsule from Orostachys fimbriatus (Turcz) Berger were optimized by experiments, which ensured the quality stability and reliability of the products and provided scientific theoretical basis for industrial production.
Related Articles |
Metrics
|
|
The Design of Modular Multi-structure Parking Garage
Collect
LI Xin-shu, GAO Lu, XU Shu-ping, ZHOU Xing-yu, YIN Jun, SHI Zhong-qi, CAO Bo-yu, LIU Xue-zhi
Journal of Jilin Institute of Chemical Technology, 2019, 36(1): 25-28.
doi:10.16039/j.cnki.cn22-1249.2019.01.006
The product is designed with multiple transmission structures such as screw drive, hydraulic drive and crank slide mechanism. It only covers two Spaces and can park six cars at the same time. With the advantages of simple structure, convenient operation and safe use, it is suitable for the old community without underground parking lot.
Related Articles |
Metrics
|
|
Numerical Analysis of Two-phase Flow of DMFC Anode Based on Fluent
Collect
CHEN Hai-lun, TIAN Ai-hua
Journal of Jilin Institute of Chemical Technology, 2019, 36(1): 29-35.
doi:10.16039/j.cnki.cn22-1249.2019.01.007
Exhausting CO2 in time and effective transferring of methanol solution to the diffusion layer have important influence on the performance of the liquid feed direct methanol fuel cell (direct methanol fuel cell, DMFC). VOF has been used to study the evolution of CO2 gas which leaked from the parallel channel, including growth, deformation, detachment and motion of the bubble. A three-dimensional model of channel has been established to study the effect of wettability on bubble evolution in channel. The software FLUENT was used to simulate and analyze the diffusion layer wall surface of hydrophilic (35o), neutral (90o),weak hydrophobic (115o) and strong hydrophobic (125o)。The analysis results show that the bubble is jointly by the pressure difference between the two phases, and surface tension effect as well. The surface of the weak hydrophobic diffusion layer is conducive to the process of bubble separation and bubble coalescence, that is, it showed bubble discharging is more stable compared with the hydrophilic surface, while smaller bubble volume and shorter escaping time compared with the strong hydrophobic surface.
Related Articles |
Metrics
|
|
Analysis of Fire Hazard in A University Dormitory Based on Fault Tree Analysis
Collect
Peng Fei, Shi Na-li
Journal of Jilin Institute of Chemical Technology, 2019, 36(1): 43-47.
doi:10.16039/j.cnki.cn22-1249.2019.01.009
With the enrollment expansion in colleges and universities in China, the number of school students increasing, more and more college students' dormitory building also.Due to the improvement of living conditions, school supplies and living things growing.The hidden danger of fire accidents will increase gradually, once fire accident happened, will directly damage the national and personal property, and life safety threat to students, seriously affect the normal teaching and living order of the school. The fire accident causes are diverse, through the fault tree qualitative and quantitative analysis the influence of various factors on the students' dormitory fire accident size,?to develop students' dormitory fire accident preventive measures has certain guiding significance.This paper takes a College dormitory 5 as an example, using fault tree analysis of the causes and consequences of the dormitory fire accident,and corresponding preventive measures are put forward.Analysis results show that the fire alarm delay, delay the time, found that don't timely, inadequate fire, fire control facilities of the failure is the most pressing problems,While other problems need to improve in peacetime work somewhat can be well improved.In addition, the corresponding fire prevention measures, the probability of fire accidents will be greatly reduced.
Related Articles |
Metrics
|
|
Glutinous Corn Convenient Porridge Development
Collect
JIE Hui, SHEN Xiao-xi, WANG Yi, JIANG Xin-yue, DONG Yao
Journal of Jilin Institute of Chemical Technology, 2019, 36(1): 48-51.
doi:10.16039/j.cnki.cn22-1249.2019.01.010
Take glutinous corn, red bean, peanut, oat, glutinous rice as raw material. It was determined by single factor experiment that corn ballon, red bean and peanut needed to be soaked for 6h and red bean for 8h. Precook glutinous corn and peanuts for 50min, glutinous rice and oats for 30min, and red beans for 60min. The optimum technological conditions were obtained by orthogonal experiment: the ratio of raw material to water was 1:16, the cooking time was 25min, and the amount of added sugar was 25% of the raw material. The corn convenient congee developed by this process has a moderate viscosity, soft taste, moderate sweetness and strong corn flavor.
Related Articles |
Metrics
|
|
Identification of Ranae and Oviductus Ranae by application of cytB in Mitochondrial DNA
Collect
DONG Yao, QIAN Yuan-mei, SONG Man, CHANG Di, CUI Hao
Journal of Jilin Institute of Chemical Technology, 2019, 36(1): 52-57.
doi:10.16039/j.cnki.cn22-1249.2019.01.011
Objective: The mitochondria DNA was employed to constructing the identified method of Oviductus Ranae by PCR. Methods: The total DNA of the adult female frog oil and the fresh issues of frog was extracted by the kit; the cytB of Rana dybowskii, Rana chensinensis, Pelophylax nigromaculatus Yamaguchi, Bufo raddei was used as the template to design four pairs of primers, and the PCR system contained above DNA and primers and the products was extracted and sequenced. Results: The DNA fragment only gained from the system contained Rana dybowskii primers and the sequence showed the identified in 99% which illustrated the experimental materials were from the Rana dybowskii. Discussion: Taking advantage of mtDNA and applying the PCR, the identified method of Oviductus Rana was established, and this can provide theory basis for the identification of Rana and Oviductus Rana.
Related Articles |
Metrics
|
|
The Research of Modeling Problems Based on the Medical Experimental Design
Collect
PAN Shu-xia, SUN Wang-jie, WU Xi, ZHANG Ruo-dong, LV Chuang, HUO Jun-shuang, NIU Xin-yu
Journal of Jilin Institute of Chemical Technology, 2019, 36(1): 62-65.
doi:10.16039/j.cnki.cn22-1249.2019.01.013
Objective:In order to exploring new ways of accurately applying models for clinical practice. Method: This paper selects orthogonal and uniform experimental designs which are commonly used in medicine to establish different models, on the basis of goodness of fit test and difference examination to judge the model. Result: Different experimental designs for the same purpose have different models. Conclusion:The same experimental purpose and experimental design, according to the goodness of fit test and difference examination, the best model can be explored by combining professional knowledge and preliminary experiment.
Related Articles |
Metrics
|
|
Study on Stability of Epidemic Model with Vaccination and Nonlinear Infectious Force
Collect
TONG Shan-shan, ZHANG Zen-yu
Journal of Jilin Institute of Chemical Technology, 2019, 36(1): 83-86.
doi:10.16039/j.cnki.cn22-1249.2019.01.018
A class of SEIR infectious disease model with inoculation is studed, and obtains the threshold condition of the existence of various equilibrium points. By using Liapunove function, Lasalle invariance principle, Hurwith criterion is proved when the basic reproduction number is less than one, the disease-free equilibrium is globally asymptotically stable;when the basic reproduction number is greater than one, this model has two equilibria, the disease-free equilibrium is unstable, discriminant analysis proved the local asymptotic stability of the equilibrium point local disease by Hurwitz, further using the theory of matrix composite track stability and global asymptotic stability of the endemic equilibrium is proved. Finally, the model is simulated, and the effect of vaccination on the epidemic is analyzed, and the main conclusions are verified in this paper.
Related Articles |
Metrics
|
|
Empirical Likelihood Inference for Integer Value Auto-regressive Model Based on Binomial Thinning Operator
Collect
ZHANG Qing-chun, LI Xiao-mei, FAN Xiao-dong
Journal of Jilin Institute of Chemical Technology, 2019, 36(1): 90-93.
doi:10.16039/j.cnki.cn22-1249.2019.01.020
Integer value time series appear in many fields such as transportation, finance, education, environment, and insurance. The thinning operator is the main method to study the integer value time series.In this paper, the first-order integer value autoregressive model based on binomial thinning operator is studied by the empirical likelihood method, and the empirical likelihood inference of the BINAR(1) model with the Poisson innovation and its empirical likelihood estimation are given. The performance of empirical likelihood estimation is studied by means of numerical simulation. Finally, the application of the model is given through an example of crime data.
Related Articles |
Metrics
|
|