鱼骨状一维链结构配位聚合物Cu(C10H14N4)(C7H4O3)2·3H2O的合成与晶体结构

doi:10.16039/j.cnki.cn22-1249.2018.07.013

Journal of Jilin Institute of Chemical Technology, 2018, 35 (7): 57-60 doi: 10.16039/j.cnki.cn22-1249.2018.07.013

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Synthesis and crystal structure of Cu(C₁₀H₁₄N₄)(C₇H₄O₃)₂·3H₂O: A coordination polymer with fish bone-like 1D chain

QU Xiao-shu,SHI Dan,LI Yan,YANG Yan-yan

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Abstract A novel coordination polymer ofCu(C₁₀H₁₄N₄)(C₇H₄O₃)₂·3H₂O (1) (C₁₀H₁₄N₄ = 1,1'-(1,4-butanediyl) bis (imidazole) (bbi); C₇H₄O₃= p-hydroxybenzoic acid) has been synthesized by convenient aqueous solution method and structurally characterized by single-crystal X-ray diffraction, powder X-ray diffraction, IR spectra and TG analysis. Single-crystal X-ray analysis reveals that the title compound is crystallized in the monoclinic system, space group R-3c with a = 20.614(19)?, b = 12.349(11)?, c = 12.003(11)?, α = 90°, β = 116.840(14)°, γ = 90°, V = 2726(4)?3, Z = 4, F(000) = 1892, S = 1.054, R1 = 0.1044, wR2 = 0.2062 [I>2σ(I)].

Published: 25 July 2018

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	QU Xiao-shu
	SHI Dan
	LI Yan
	YANG Yan-yan

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QU Xiao-shu,SHI Dan,LI Yan, et al. Synthesis and crystal structure of Cu(C₁₀H₁₄N₄)(C₇H₄O₃)₂·3H₂O: A coordination polymer with fish bone-like 1D chain[J]. Journal of Jilin Institute of Chemical Technology, 2018, 35(7): 57-60.

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https://xuebao.jlict.edu.cn/EN/10.16039/j.cnki.cn22-1249.2018.07.013 OR https://xuebao.jlict.edu.cn/EN/Y2018/V35/I7/57