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吉林化工学院学报, 2018, 35(7): 48-52     https://doi.org/10.16039/j.cnki.cn22-1249.2018.07.011
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基于D101C大孔吸附树脂的原人参三醇组皂苷的分离研究
成乐琴,张跃伟,李延春,李玲,孙硕
吉林化工学院 化学与制药工程学院;吉林省彩森仁生物科技有限责任公司
Study on the Isolation of Protopanaxatriol Type Saponins based on D101C Macroporous Adsorption Resin
Cheng Le-qin,Zhang Yue-wei,Li Yan-chun,Li Ling,Sun Shuo
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摘要 原人参三醇组皂苷(简称PPT型皂苷)是人参中主要的两种四环三萜皂苷之一,在人参茎叶中含量相对较高,具有抗疲劳、抗应激等功效。本文以人参茎叶总皂苷为原料,研究了人参茎叶总皂苷浓度、吸附温度、吸附时间对D101C大孔吸附树脂对PPT型皂苷和PPD型皂苷的吸附影响,同时考察了乙醇浓度对D101C大孔吸附树脂解吸PPT型皂苷和PPD型皂苷的影响。实验结果表明:利用D101C大孔吸附树脂在15 ℃温度下吸附浓度为15 mg/mL的人参茎叶总皂苷14 h,再利用45%的乙醇水溶液于25 ℃解吸14 h人参茎叶皂苷时, PPT型皂苷的含量由原来的27.2%提高到86.8%,PPT型皂苷:PPD型皂苷由1.1:1提高到185:1,显示出良好的PPT皂苷的分离及提纯效果。
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成乐琴
张跃伟
李延春
李玲
孙硕
关键词:  PPT型皂苷  PPD型皂苷  D101C大孔吸附树脂  分离    
Abstract: Protopanaxatriol group (PPT) is one of the two major tetracyclic triterpenoid saponins, responsible for anti-fatigue, anti-stress effects. This report studied the influence on adsorption of total PPT and PPD on D101C macroporous resin, by factors including concentration of total ginsenosides in stem and leaf, temperature and time of adsorption. In addition, influence of ethanol percentage was evaluated for desorption. Experimental results demonstrates that D101C microporous adsorption resin can adsorb 15 mg/mL of total ginsenosides at 15 ℃ after 14 hours, with PPT content further elevated to 86.8% from 27.2% and increased ratio of PPT to PPD (185:1 from 1.1:1) by desorption of 45% ethanol at 25 ℃ for 14 hours, indicating a better extraction and purification method of isolation and purification.
Key words:  PPT saponin    PPD saponins    D101C microporous adsorption resin    isolation
               出版日期:  2018-07-25      发布日期:  2018-07-25      整期出版日期:  2018-07-25
R282.1  
引用本文:    
成乐琴, 张跃伟, 李延春, 李玲, 孙硕. 基于D101C大孔吸附树脂的原人参三醇组皂苷的分离研究[J]. 吉林化工学院学报, 2018, 35(7): 48-52.
Cheng Le-qin, Zhang Yue-wei, Li Yan-chun, Li Ling, Sun Shuo. Study on the Isolation of Protopanaxatriol Type Saponins based on D101C Macroporous Adsorption Resin. Journal of Jilin Institute of Chemical Technology, 2018, 35(7): 48-52.
链接本文:  
https://xuebao.jlict.edu.cn/CN/10.16039/j.cnki.cn22-1249.2018.07.011  或          https://xuebao.jlict.edu.cn/CN/Y2018/V35/I7/48
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