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| Hydrothermal Synthesis and crystal structure of Cu12Cl2(trz)8[HPMo12O40]]n |
| YU Xiao-yang,LUO Ya-nan,QU Xiao-shu,YANG Yan-yan,REN Hong,JIN Li
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Abstract A new polyoxometalates compound, Cu12Cl2(trz)8[HPMo12O40]]n （1）（trz = 1,2,4-1H-triazole）, has been synthesized under hydrothermal condition and characterized by elemental analysis, IR and single crystal X-ray diffraction. It crystallizes in the monolinic system, space group C2/m, a = 2.1618(4) nm, b = 2.16726(10) nm, c = 1.60124(15) nm, β = 117.090(11)°, V = 6.3207(14) nm3, Z = 4. In addition, the fluorescence property of compound 1 was also investigated.
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Published: 25 July 2018
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