聚酚抗氧化剂CPL改性研究

doi:10.16039/j.cnki.cn22-1249.2018.07.006

摘要
相关文章
推荐阅读
Metrics

下载:

PDF (458KB)
输出: BibTeX | EndNote (RIS)

摘要本文探索了聚酚抗氧化剂改性的新方法。以丙烯酸、三氯氧磷、三乙胺等为反应原料，通过酯化法合成CPL酯化物，进行对比实验，采用单因素实验法，确定了合成的最佳工艺条件为：m（聚酚化合物）：m（丙烯酸）：m（三氯氧磷）：m（三乙胺）=18：2：4：3，最佳反应温度为79℃，保温反应时间2.5h，在此工艺条件下，酯化率可达88.0～90.0%。

	服务
	把本文推荐给朋友
	加入引用管理器
	E-mail Alert
	RSS
	（）
	作者相关文章
	高瑀婷
	戴传波

关键词: 聚酚抗氧化剂酯化法改性

Abstract: A new method of modification of polyphenol antioxidant was explored. CPL esterification was synthesized by esterification with acrylic acid, phosphorus oxychloride and triethylamine. A single factor experiment was carried.The optimum process conditions are as follows: m (polyphenol compound): m (acrylic acid): m (phosphorus oxychloride): m (triethylamine) =18:2:4:3, the optimum reaction temperature is 79℃, and the heat preservation reaction time is 2.5h. Under this technological condition, esterification. The esterification rate 88 to 90%.

Key words: polyphenol antioxidants esterification modification

出版日期: 2018-07-25 发布日期: 2018-07-25 整期出版日期: 2018-07-25

TQ460

引用本文:

高瑀婷, 戴传波. 聚酚抗氧化剂CPL改性研究[J]. 吉林化工学院学报, 2018, 35(7): 26-28.
Gao Yuting, Dai Chuanbo. Study on the modification of isobutylated products of P - methylphenol dicyclopentadiene. Journal of Jilin Institute of Chemical Technology, 2018, 35(7): 26-28.

链接本文:

https://xuebao.jlict.edu.cn/CN/10.16039/j.cnki.cn22-1249.2018.07.006 或 https://xuebao.jlict.edu.cn/CN/Y2018/V35/I7/26

[1]	韩雨桐, 刘嘉欣, 吕宏洋, 沈启慧, 刘岩. 乌拉草还原纳米银对亚麻羊毛织物改性处理 [J]. 吉林化工学院学报, 2024, 41(7): 1-6.
[2]	陈龙溪l, 孟祥佳, 王进芳, 刘姿秀, . 高纯空气介质阻挡辉光放电对双向拉伸聚丙烯薄膜表面改性研究 [J]. 吉林化工学院学报, 2023, 40(9): 16-22.
[3]	董林辉, 孟凡飞, 宋鹏, 邱俊. 催化剂ZrO2/Na-β和ZrO2/H-β的制备及其催化环己酮和异丙醇MPV反应的性能 #br# [J]. 吉林化工学院学报, 2023, 40(7): 11-18.
[4]	巩振虎, 刘义章, 周凯, 王仕亮. TiO₂光催化剂的改性与应用 [J]. 吉林化工学院学报, 2021, 38(9): 102-106.
[5]	李格乐, 王润霖, 吴小康, 王颖, 翦英红. 餐余地沟油固化过程中的脱酸处理研究 [J]. 吉林化工学院学报, 2020, 37(5): 70-74.
[6]	林明穗, 张昌婷, 赵炎, 罗菊香, 苏志忠. ABS接枝马来酸酐增容ABS/PMMA复合材料机械性能及形貌分析 [J]. 吉林化工学院学报, 2019, 36(3): 69-73.
[7]	白鹭, 吴春英, 谷风, 陆文龙. 氢氧化铁胶体改性聚偏氟乙烯膜的制备及性能研究[J]. 吉林化工学院学报, 2018, 35(5): 83-86.

[1]	WANG Weina. The Method for Portrait Depiction of Members in Department Stores based on Fuzzy Clustering and RFM Model [J]. Journal of Jilin Institute of Chemical Technology, 2019, 36(11): 71 -73 .
[2]	JING Chunyou. Research on the Construction of All-Round Education Mechanism in Universities Based on the Tutorial System for Teacher Party Members [J]. Journal of Jilin Institute of Chemical Technology, 2019, 36(12): 6 -9 .
[3]	GAO Jingnan, WU Jingjie. On the Ways of Improving the Sense of Acquisition of Ideological and Political Theory Course for College Students [J]. Journal of Jilin Institute of Chemical Technology, 2019, 36(12): 38 -41 .
[4]	HAN Yun-hua, SHI Lei. Study on Synthesis of Polyol Acrylate[J]. Journal of Jilin Institute of Chemical Technology, 2018, 35(1): 4 -7 .
[5]	WANG Ya-hong, JIA Ying-chao. Optimization for Soxhlet Extraction of Total Flavonoids from Eggplant Root by Using Response Surface Methodology[J]. Journal of Jilin Institute of Chemical Technology, 2018, 35(3): 1 -6 .
[6]	ZENG Xiao-dan, JIANG Cheng, XI Hao, ZHU Lin. The Study of Determination of Carbon Tetrachloride Divergence in the Chlorosulfonated Polyethylene (CSM) Production Process[J]. Journal of Jilin Institute of Chemical Technology, 2018, 35(1): 8 -12 .
[7]	PAN Hong-wei, ZHOU Hong-li. Research Progress on Extraction Technology and Component Analysis of Volatile Flavor Compounds in Plants[J]. Journal of Jilin Institute of Chemical Technology, 2018, 35(3): 7 -10 .
[8]	YAN Zhen-han, CHEN Qing. Analysis of Pressure Sealing Technology Research[J]. Journal of Jilin Institute of Chemical Technology, 2018, 35(3): 11 -14 .
[9]	SUN Xiao-feng, YU Wen-xin, ZHU Ming-wei, JIE Meng, JIANG De-lon. Research on the Piezoelectric Pump Application in Continuous Ink Supply System of the Inkjet Printer[J]. Journal of Jilin Institute of Chemical Technology, 2018, 35(3): 15 -18 .
[10]	LIU Haiyong. The Influence of the Mobile Internet Technology on Ideological and Political Classroom Teaching---A Periodical Reflection on the Teaching Effectiveness Based on instructional software [J]. Journal of Jilin Institute of Chemical Technology, 2019, 36(12): 42 -45 .

Viewed

Full text

Abstract

Cited

Shared

Discussed