X射线荧光光谱法辅助测定重晶石中的硫酸钡
孙杨,李冬梅,刘茜,苏丹,刘岩,沈启慧
吉林化工学院 化学与制药工程学院,吉林省有色金属地质勘查局测试中心
Determination of Barium Sulfate in Barite by X-ray Fluorescence Spectrometry
SUN Yang,LI Dong-mei,LIU Qian,SU Dan,LIU Yan,SHEN Qi-hui
摘要 重晶石通过王水和氢氟酸溶解可溶性盐、蒸干除去硅,用盐酸浸取,再经过滤、充分洗涤和灼烧恒重,快速获得硫酸钡和硫酸锶的总量。通过X射线荧光光谱无差减标样分析法测定硫酸锶含量后,即通过计算得到硫酸钡含量。本法简单、快速、效率高。
关键词:
X射线荧光光谱法
无标分析
重量法
重晶石
硫酸钡
Abstract: Barite dissolved by aqua regia and hydrofluoric acid soluble salt, dried to remove silicon by hydrochloric acid leaching, and then through filtering, washing and burning constant weight, quick got the amount of barium sulphate and strontium sulphate. Through the X-ray fluorescence spectrometry, the content of strontium sulfate was determined by the calculation of barium sulfate. This method was simple, fast, and efficient.
Key words:
X-ray fluorescence spectrometry
UniQuant
weight method
barite
barium sulfate
出版日期: 2018-05-25
发布日期: 2018-05-25
整期出版日期: 2018-05-25
引用本文:
孙杨, 李冬梅, 刘茜, 苏丹, 刘岩, 沈启慧. X射线荧光光谱法辅助测定重晶石中的硫酸钡[J]. 吉林化工学院学报, 2018, 35(5): 27-29.
SUN Yang, LI Dong-mei, LIU Qian, SU Dan, LIU Yan, SHEN Qi-hui. Determination of Barium Sulfate in Barite by X-ray Fluorescence Spectrometry. Journal of Jilin Institute of Chemical Technology, 2018, 35(5): 27-29.
链接本文:
https://xuebao.jlict.edu.cn/CN/10.16039/j.cnki.cn22-1249.2018.05.007
或
https://xuebao.jlict.edu.cn/CN/Y2018/V35/I5/27
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