不同辅助方法对刺玫果总多酚提取率的影响

doi:10.16039/j.cnki.cn22-1249.2020.01.005

摘要
相关文章
推荐阅读
Metrics

下载:

PDF (517KB)
输出: BibTeX | EndNote (RIS)

摘要

探索不同辅助方法对刺玫果总多酚提取率的影响。通过单因素和正交试验获得传统溶剂法提取刺玫果总多酚的最佳工艺条件为：料液比1:50(g:mL)、提取溶剂为50%的乙醇溶液、提取温度80℃、提取1.5h，总多酚提取率为11.28mg/g；然后分别考察离子液体辅助、离子液体协同超声波辅助、离子液体协同超声波-微波辅助对刺玫果总多酚提取率的影响。试验结果表明，经离子液体氯化-1-丁基-3-甲基咪唑辅助提取后刺玫果总多酚的提取率较传统溶剂法提高了14.98%；经离子液体协同超声波辅助提取后刺玫果总多酚提取率提高了16.13%；经离子液体协同超声波-微波辅助提取后刺玫果总多酚提取率提高了20.66%。上述结果表明，离子液体辅助、离子液体协同超声波辅助、离子液体协同超声波-微波辅助均能提高刺玫果总多酚的提取率，为刺玫果总多酚的后续开发利用提供了试验参考。

	服务
	把本文推荐给朋友
	加入引用管理器
	E-mail Alert
	RSS
	（）
	作者相关文章
	戴鹂莹
	雷永平
	王晓林
	邸松
	钟方丽

关键词: 刺玫果总多酚离子液体超声波-微波工艺优化

Abstract:

Exploring the effects of different ancillary methods on the extraction rate of total polyphenols from Fruit of Rosa davurica Pall(FRDP). The optimum conditions for extracting the total polyphenols from FRDP were obtained by single factor and orthogonal experiments: the ratio of material to liquid 1:50 (g:mL), the extraction solvent was 50% ethanol solution, the extraction temperature was 80 °C. After extraction for 1.5 h, the total polyphenol extraction rate was 11.28 mg/g. Then the effects of ionic liquid assisted, ionic liquid synergistic ultrasonic assisted, ionic liquid synergistic ultrasonic-microwave assisted extraction on the extraction rate of total polyphenols from FRDP were investigated. The results showed that the extraction rate of total polyphenols from the ionic liquid was improved by 14.98% compared with the traditional solvent method. The ionic liquid was assisted by ultrasonic-assisted extraction. The extraction rate of total polyphenols in FRDP was increased by 16.13%. The extraction rate of total polyphenols in FRDP was increased by 20.66% by ionic liquid combined with ultrasonic-microwave assisted extraction. The above results indicated that ionic liquid assisted, ionic liquid synergistic ultrasonic assisted, ionic liquid synergistic ultrasonic-microwave assisted can increase the extraction rate of total polyphenols from FRDP, and provide a test reference for the subsequent development and utilization of total polyphenols.

Key words: Ruit of Rosa davurica Pall total polyphenols Ionic liquids ultrasonic-microwave process optimization

出版日期: 2020-01-25 发布日期: 2020-01-25 整期出版日期: 2020-01-25

ZTFLH:

TS201

引用本文:

戴鹂莹, 雷永平, 王晓林, 邸松, 钟方丽. 不同辅助方法对刺玫果总多酚提取率的影响 [J]. 吉林化工学院学报, 2020, 37(1): 20-24.
DAI Liying, LEI Yongping, WANG Xiaolin, DI Song, ZHONG Fangli. Effects of Different Auxiliary Methods on the Extraction Rate of Total Polyphenols from Fruit of Rosa Davurica Pall . Journal of Jilin Institute of Chemical Technology, 2020, 37(1): 20-24.

链接本文:

http://xuebao.jlict.edu.cn/CN/10.16039/j.cnki.cn22-1249.2020.01.005 或 http://xuebao.jlict.edu.cn/CN/Y2020/V37/I1/20

[1]	赵鹤鹏, 刘佳南. 响应面法优化微波辅助提取沙棘籽油的工艺研究 [J]. 吉林化工学院学报, 2019, 36(11): 17-21.
[2]	王宗勇, 赵轶, 何苗, 杨慧茹, 李萍, 薛晓丽. 超临界CO₂流体萃取木耳菌糠最佳工艺的研究 [J]. 吉林化工学院学报, 2019, 36(1): 5-10.
[3]	宋健刚, 钟方丽, 王晓林, 林宇. 离子液体超声辅助提取黑果腺肋花楸果中花青素的工艺研究 [J]. 吉林化工学院学报, 2018, 35(9): 24-31.
[4]	刘金璐, 雷永平, 王晓林, 钟方丽. 刺玫果总皂苷的纯化工艺及体外活性研究 [J]. 吉林化工学院学报, 2018, 35(9): 16-23.
[5]	杨艳俊, 王亚红, 杨秀东. 表面活性剂辅助提取水蜈蚣总多酚的工艺优化 [J]. 吉林化工学院学报, 2018, 35(9): 11-15.
[6]	蒋云霞, 徐百灵, 陈丽娜, 徐杰. 含联苯基团的咪唑类离子液体的微波合成[J]. 吉林化工学院学报, 2018, 35(7): 53-56.

[1]	YANG Xian-wei, ZHAN Xue-qiu, KANG Hong-juan, LUO Ying. A Method of Analyzing Image Abnormality by Quadratic Sieve [J]. Journal of Jilin Institute of Chemical Technology, 2018, 35(9): 70 -75 .
[2]	PANG Jia-bao. An Analysis of the Development and Protection of King Ross's Royal Palace in Qianguo [J]. Journal of Jilin Institute of Chemical Technology, 2018, 35(12): 86 -88 .
[3]	ZHOU Li-yuan. To Promote Regional Resource Sharing on the Basis of Resource Security: Research on Library Service Socialization in Universities in Jilin City [J]. Journal of Jilin Institute of Chemical Technology, 2018, 35(12): 103 -106 .
[4]	SONG Chunlei, WANG Kaibao, HOU Daibing, GUO Wenqi, QIN Qingkun, PAN Leiting, CHI Mingtian. Wearable Ski Equipment Sterilizer Analysis of Scheme and Structure Design and Disinfection Effect [J]. Journal of Jilin Institute of Chemical Technology, 2019, 36(3): 34 -37 .
[5]	LI Xin, ZHAN Dechen. A Study on the Teaching Mode Reform of University Computer Course [J]. Journal of Jilin Institute of Chemical Technology, 2019, 36(6): 27 -31 .
[6]	SHANG Yuying, ZHANG Meili, GAO Dan. A Diagonal Iterative Algorithm for the Spectral Radius of a Nonnegative Matrix [J]. Journal of Jilin Institute of Chemical Technology, 2019, 36(7): 86 -90 .
[7]	ZHENG QingLan. Design of AC Charging Pile System for Electric Vehicles [J]. Journal of Jilin Institute of Chemical Technology, 2019, 36(9): 44 -50 .
[8]	LI Shungyuan, WANG Qinmin. Design and Implementation of Laboratory Access Control System Based on Face Recognition [J]. Journal of Jilin Institute of Chemical Technology, 2019, 36(9): 82 -85 .
[9]	WU Hanyang. Research on alumni donation behavior of local colleges [J]. Journal of Jilin Institute of Chemical Technology, 2019, 36(12): 83 -86 .
[10]	ZU Guojing, LU Hehuan, WU Lishun, TONG Qingsong. Preparation and Adsorption Properties of Polyvinyl Alcohol Polyacrylamide Interpenetrating Polymer Network Hydrogel [J]. Journal of Jilin Institute of Chemical Technology, 2020, 37(1): 1 -7 .

Viewed

Full text

Abstract

Cited

Shared

Discussed